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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2423052Generated: November 1, 2026

Benzenamine, 2-chloro-5-(trifluoromethyl)- → HCID 923997, compound

https://huagongshe.com/reaction/2423052

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzenamine, 2-chloro-5-(trifluoromethyl)-HCID 8475—
Reactant2-ChlorobenzimidazoleHCID 78572—
ProductHCID 923997HCID 923997—

Reaction Steps

The title compound was prepared from 2-chlorobenzimidazole and 3-amino-4-chlorobenzotrifluoride by Procedure A. The product was isolated upon basic work-up and purified by preparative LCMS to give the title compound as the free base. 1NMR (CDCl3) δ 6.40 (br s, 2H), 7.11-7.15 (d, 1H), 7.18-7.25 (m, 2H), 7.35-7.41 (d, 1H), 7.42-7.46 (m, 2H), 8.57 (s, 1H). MS(ES+) m/z 312 ([M+1]+, 100).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07960561B2
Source datasetuspto-grants-2011_06
ORD IDord-a83138a6ebee4cd2865c636a1980fd9b
Source noteuspto-grants-2011_06