HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 2-chloro-5-(trifluoromethyl)- → HCID 923997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 2-chloro-5-(trifluoromethyl)- | HCID 8475 | — |
| Reactant | 2-Chlorobenzimidazole | HCID 78572 | — |
| Product | HCID 923997 | HCID 923997 | — |
Reaction Steps
The title compound was prepared from 2-chlorobenzimidazole and 3-amino-4-chlorobenzotrifluoride by Procedure A. The product was isolated upon basic work-up and purified by preparative LCMS to give the title compound as the free base. 1NMR (CDCl3) δ 6.40 (br s, 2H), 7.11-7.15 (d, 1H), 7.18-7.25 (m, 2H), 7.35-7.41 (d, 1H), 7.42-7.46 (m, 2H), 8.57 (s, 1H). MS(ES+) m/z 312 ([M+1]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960561B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-a83138a6ebee4cd2865c636a1980fd9b |
| Source note | uspto-grants-2011_06 |