HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 178513298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 3-Cyanobenzoic acid | HCID 15875 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178513298 | HCID 178513298 | — |
Reaction Steps
An aqueous 50% hydroxylamine solution was added to a methanol solution of 3-cyanobenzoic acid, followed by heating under reflux for 11 hours. The reaction liquid was concentrated, diluted with water, adjusted with 1 M hydrochloric acid to have a pH of from 2 to 3, and the precipitate was collected by filtration to obtain 3-[(hydroxyamino)(imino)methyl]benzoic acid. ES+: 181.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960562B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-3981e0f0009a4b3eb4f2c690e29dce2a |
| Source note | uspto-grants-2011_06 |