HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59864897, compound → HCID 59864864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59864897 | HCID 59864897 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59864864 | HCID 59864864 | — |
Reaction Steps
Compound 19.3 (230 mg, 0.53 mmol) was dissolved in mixture of ethyl acetate (3 mL) and methanol (1 mL). 10% Pd/C (56 mg, 0.053 mmol) was added and the reaction mixture was stirred for 1.5 h under H2 at room temperature. The reaction mixture was filtered, the residue concentrated under reduced pressure to afford 19.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960567B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-453cb26558614bbeb124dd9ed37f28c9 |
| Source note | uspto-grants-2011_06 |