HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59864784, compound → HCID 59864822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59864784 | HCID 59864784 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59864822 | HCID 59864822 | — |
Reaction Steps
Pd/C (30 mg) was added to 25.2 (250 mg) in EtOH (15 mL). The mixture was stirred under hydrogen at room temperature for 6 h. The catalyst was removed by filtration through celite. The filtrate was concentrated under vacuum to give 25.3. MS ESI (pos.) m/z: 369.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960567B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-21d0fa7938b0411a923dee681c029492 |
| Source note | uspto-grants-2011_06 |