HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 67245786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 67243224 | HCID 67243224 | — |
| Catalyst | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 67245786 | HCID 67245786 | 100% |
Reaction Steps
(3-Iodo-4-methanesulfonylamino-5-methylbenzyl)carbamic acid t-butyl ester (122.0 mg, 0.27 mmol) and CF3COOH (5˜6 drops) were added into methylene chloride. The mixture was stirred for 12 hrs. The mixture was concentrated in vacuo to yield brownish syrup (142.2 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07960584B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-5d3dd03467844084a740d5c0e54a7c29 |
| Source note | uspto-grants-2011_06 |