Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178424441 | HCID 178424441 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23677956 | HCID 23677956 | 100.3% |
Reaction Steps
0.18 mL (0.36 mmol) of 2 mol/L aqueous sodium hydroxide solution was added to an ethanol (2 mL) solution containing 100 mg (0.361 mmol) of 6-chloro-3-(2-cyclo-propyl-6-methylphenoxy)-4-pyridazinol, and the resulting mixture was stirred at 50° C. for 4 hours. The reaction mixture was concentrated to obtain 108 mg (0.361 mmol, Yield: 100%) of sodium 6-chloro-3-(2-cyclopropyl-6-methyl-phenoxy)-4-pyridazinolate (Compound No. 3805).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07964531B2 |
|---|
| Source dataset | uspto-grants-2011_06 |
|---|
| ORD ID | ord-23c41a8e4a03421b92e612a399aed769 |
|---|
| Source note | uspto-grants-2011_06 |
|---|