HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-tert-Butylisophthalic acid → 5-Tert-butyl isophthalic acid 2-ethyl-4-methylimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-tert-Butylisophthalic acid | HCID 75379 | — |
| Reactant | HCID 178437635 | HCID 178437635 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-Tert-butyl isophthalic acid 2-ethyl-4-methylimidazole | HCID 178441090 | — |
Reaction Steps
To a 3 L-three neck flask, 180.0 g of 5-tert butyl isophthalic acid and 107.1 g of 2-ethyl-4-methylimidazole, and 810 ml of methanol were added, stirred and heated at reflux for 3 hours. After cooling, by performing filtration and vacuum drying, 201.3 g of the clathrate complex of 5-tert-butyl isophthalic acid/2-ethyl-4-methylimidazole (1:1) was obtained. The clathration of the obtained clathrate complex was confirmed by 1H-NMR, TG-DTA and XRD.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653160B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-1b6bbaae4eee480daa7852b2bc972542 |
| Source note | uspto-grants-2014_02 |