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HRID242510

反应详情

EQUATION

反应方程式

HRID 242510 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(C(=O)O)c2ccccc12
HCID69065

1,4-Naphthalenedicarboxylic acid

C12H8O4

结构：CCCCCCCCCCCc1ncc[nH]1
HCID85582

1H-Imidazole, 2-undecyl-

C14H26N2

PRODUCTS

生成物

1
结构：CCCCCCCCCCCc1ncc[nH]1.O=C(O)c1ccc(C(=O)O)c2ccccc12
HCID68635264

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

To a 3 L-three neck flask, 43.2 g of 1,4-naphthalenedicarboxylic acid and 44.5 g of 2-undecylimidazole, and 1000 ml of ethyl acetate were added, stirred and heated at reflux for 3 hours. After cooling, by performing filtration and vacuum drying, 85.9 of the clathrate complex of 1,4-naphthalenedicarboxylic acid/2-undecylimidazole (1:1) was obtained. The obtained clathrate complex was subjected to 1H-NMR, TG-DTA and XRD to confirm the clathration.

WORKUP

后处理

  1. temperatureheated
  2. temperatureat reflux for 3 hours
  3. temperatureAfter cooling
  4. filtrationfiltration and vacuum
  5. customdrying