1,4-Naphthalenedicarboxylic acid → 1,4-Naphthalenedicarboxylic acid 2-undecylimidazole

Beteiligte Stoffe

Reaktionsschritte

To a 3 L-three neck flask, 43.2 g of 1,4-naphthalenedicarboxylic acid and 44.5 g of 2-undecylimidazole, and 1000 ml of ethyl acetate were added, stirred and heated at reflux for 3 hours. After cooling, by performing filtration and vacuum drying, 85.9 of the clathrate complex of 1,4-naphthalenedicarboxylic acid/2-undecylimidazole (1:1) was obtained. The obtained clathrate complex was subjected to 1H-NMR, TG-DTA and XRD to confirm the clathration.

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