2,4-Difluorophenylboronic acid → HCID 11508373, compound

Participants

Reaction Steps

Using a method analogous to that described in Example 40, 4-bromophenyl-sulfonic acid-(4-hydroxybutyl)-amide and 2,4-difluorophenyl boronic acid were reacted to give the title compound as a white solid. δC (CDCl3, 62.9 MHz): 25.9, 29.6, 42.6, 60.2, 104.7 (t, J 25.8), 112.0 (dd, J 22.9 and 3.5), 127.3, 129.6, 131.5 (d, J 8.8), 131.5 (d, J 9.8), 139.1, 139.4, 159.9 (dd, J 252.0, 11.7) and 163.0 (dd, J 252.0, 11.7).

Provenance & Evidence