m-Bromobenzenesulphonyl chloride → HCID 67245018, compound
Reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([S:8](Cl)(=[O:10])=[O:9])[CH:5]=[CH:6][CH:7]=1.[NH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][OH:18]>>[OH:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][NH:12][S:8]([C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([Br:1])[CH:3]=1)(=[O:10])=[O:9]Participants
3
Procedure
Using a method analogous to that described in Example 1, 3-bromophenyl sulphonyl chloride was reacted with 5-aminopentanol, and the title compound obtained as a white solid after recrystallisation from ether/petrol.
Sources & evidence
- ORD record
- ord-a1aefdebe6b643f693cb304e972e6f95
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07964643B2
Reaction notes
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