HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Nitrophenyl)boronic acid → HCID 11538968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Nitrophenyl)boronic acid | HCID 2773548 | — |
| Reactant | 4-Bromo-N-(4-hydroxybutyl)-2-(trifluoromethyl)benzene-1-sulfonamide | HCID 16094726 | — |
| Product | HCID 11538968 | HCID 11538968 | — |
Reaction Steps
Using a method analogous to that described in Example 40, 4-bromo-2-trifluoromethylphenyl-sulfonic acid-(4-hydroxybutyl)-amide and 2-nitrophenyl boronic acid were reacted to give the title compound as a thick oil. δC (DMSO, 62.9 MHz): 26.1, 29.5, 42.8, 60.2, 128.2, 124.9, 120.7, 128.7, 130.2, 132.6, 133.1, 133.5, 139.3, 139.8, 141.8 and 147.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964643B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-77f90c16167444acbb660f48489a5fa8 |
| Source note | uspto-grants-2011_06 |