N-(tert-butoxycarbonyl)glycine → HCID 67245336, compound
Reaction equation
C(OC([NH:8][CH2:9][C:10](O)=[O:11])=O)(C)(C)C.[ClH:13].[C:14]1([CH:20]([NH2:31])[C:21]2[CH:26]=[CH:25][C:24]([C:27]([F:30])([F:29])[F:28])=[CH:23][CH:22]=2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[ClH:13].[NH2:8][CH2:9][C:10]([NH:31][CH:20]([C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)[C:21]1[CH:26]=[CH:25][C:24]([C:27]([F:29])([F:30])[F:28])=[CH:23][CH:22]=1)=[O:11]Participants
3
Procedure
Prepared in analogy to example 3.1, starting from N-tert.butyloxycarbonyl glycine and C-phenyl-C-(4-trifluoromethyl-phenyl)-methylamine hydrochloride (CA [49703-60-8]).
Workup
- customPrepared in analogy to example 3.1
Sources & evidence
- ORD record
- ord-5f7dcb0032704cc788305f52069239ce
- Source dataset
- uspto-grants-2011_06
- Patent number
- US07964645B2
Reaction notes
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