Bromine → HCID 87322888, compound

Participants

Reaction Steps

Bromine (0.698 g) was added to a solution of 1 (1.80 g, 4.16 mmol) in CH2Cl2 (15 mL). After stirring overnight at room temperature, the mixture was neutralized with saturated aqueous NaHCO3 solution and extracted with CH2Cl2 (3×20 mL). The organic layers were combined, dried over MgSO4, and concentrated in vacuo (1.90 g, 89%).

Provenance & Evidence