Lithium Hydroxide → HCID 67246991, compound

Participants

Reaction Steps

To a solution of 6 (8 mg, 0.022 mmol) in MeOH (0.1 mL) was added LiOH (0.01 g, 0.154 mmol). The reaction was refluxed for 2 hours. The resulting solution was concentrated and purified with silica gel chromatography eluding with 75% MeOH and 25% CH2Cl2. The reaction provided 7 (2.6 mg, 0.00822 mmol, 37%).

Provenance & Evidence