Hydrochloric Acid → HCID 67248603, compound

Participants

Reaction Steps

To 10 mL of 12 M hydrochloric acid was added 5 (0.2 g, 0.451 mmol). Methanol was added until mix became homogenous and solution was allowed to reflux for 2 hours. The resulting mix was concentrated and co-evaporated with methanol and ether (3×10 mL). The reaction provided 10 (63 mg, 0.2076 mmol, 46%).

Provenance & Evidence