HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-[(2-Methylbut-3-yn-2-yl)oxy]quinoline → HCID 639605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-[(2-Methylbut-3-yn-2-yl)oxy]quinoline | HCID 59134321 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | HCID 639605 | HCID 639605 | — |
Reaction Steps
A solution of 6-[(1,1-dimethyl-2-propynyl)oxy]quinoline (16.7 mmol) in 1,2-dichlorobenzene (10 mL) was stirred at 180° C. for 1 hour. Upon the completion of the reaction, the solvent was distilled off, and the residue was recrystallized with hexane-ethyl acetate to obtain the aimed compound (2-step, quant.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964623B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-0934440df4864270884be38b3fd067a4 |
| Source note | uspto-grants-2011_06 |