HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 68424421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 67246646 | HCID 67246646 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Product | HCID 68424421 | HCID 68424421 | 98% |
Reaction Steps
To a solution of 7-methoxymethoxy-2,2-dimethyl-6-nitro-4-(2-phenylethylamino)-3,4-dihydro-2H-1-benzopyrane (265 mg, 0.66 mmol) in ethanol (5 mL), 5% palladium-carbon (AER type, 13 mg) was added at room temperature, and the resulting mixture was stirred under hydrogen stream overnight. Upon the completion of the reaction, the resulting solution was filtered through celite, concentrated, and the aimed product was obtained (yield: 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964623B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-c99fdaf319c640889039f9562197c972 |
| Source note | uspto-grants-2011_06 |