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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2425363Generated: October 28, 2026

Ethanol → HCID 68424421, compound

https://huagongshe.com/reaction/2425363

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHCID 67246646HCID 67246646—
CatalystHCID 178418390HCID 178418390—
ProductHCID 68424421HCID 6842442198%

Reaction Steps

To a solution of 7-methoxymethoxy-2,2-dimethyl-6-nitro-4-(2-phenylethylamino)-3,4-dihydro-2H-1-benzopyrane (265 mg, 0.66 mmol) in ethanol (5 mL), 5% palladium-carbon (AER type, 13 mg) was added at room temperature, and the resulting mixture was stirred under hydrogen stream overnight. Upon the completion of the reaction, the resulting solution was filtered through celite, concentrated, and the aimed product was obtained (yield: 98%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07964623B2
Source datasetuspto-grants-2011_06
ORD IDord-c99fdaf319c640889039f9562197c972
Source noteuspto-grants-2011_06