HRID2425436

反应详情

EQUATION

反应方程式

HRID 2425436 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Intermediate 38a (141 mg) obtained in Step A was dissolved in a solution of trifluoroacetic acid (0.9 ml, Aldrich) in dichloromethane (2.1 ml), and the solution was stirred at room temperature 5 hours. The solvent was evaporated under reduced pressure to obtain the title compound as trifluoroacetate (145 mg).

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure