HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 57579988, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methoxyacetic Acid | HCID 12251 | — |
| Reactant | (Boc-aminooxy)acetic acid | HCID 2755974 | — |
| Reactant | HCID 86627813 | HCID 86627813 | — |
| Product | HCID 57579988 | HCID 57579988 | — |
Reaction Steps
(S)-3-[2-(tert-Butoxycarbonylaminooxy)acetyl]amino-1-(4-chloro-5-isoquinolinesulfonyl)pyrrolidine can be prepared from hydrochloride of the compound prepared in Example 19-2 by using 2-(tert-butoxycarbonylaminooxy)acetic acid in the method of Example 56-1 instead of 2-methoxyacetic acid, and the protective group of the obtained compound can be removed according to the method described in Example 1-1, Step B to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964613B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-ef894517c1f44e7a9f629f9007866714 |
| Source note | uspto-grants-2011_06 |