HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → Trifluoroacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67243468 | HCID 67243468 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Trifluoroacetate | HCID 84468 | — |
| Product | HCID 67242571 | HCID 67242571 | — |
Reaction Steps
(S)-3-[2-[2-(Dimethylamino)ethoxy]acetyl]amino-1-(tert-butoxycarbonyl)pyrrolidine (175 mg) prepared in Step D was added with a 30% solution of trifluoroacetic acid in dichloromethane (5 ml), and the mixture was stirred at room temperature. The volatile components were removed to obtain the title compound as trifluoroacetate (246 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964613B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-cbed5dbaa1b642018138ce975f0fc9eb |
| Source note | uspto-grants-2011_06 |