HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4'-Bipiperidine → HCID 11636033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4'-Bipiperidine | HCID 78607 | — |
| Reactant | (4S,5R)-2-(4-tert-butyl-2-ethoxy-phenyl)-4,5-bis-(4-chloro-phenyl)-4,5-dihydro-imidazole-1-carbonyl chloride | HCID 57732375 | — |
| Product | HCID 11636033 | HCID 11636033 | — |
Reaction Steps
[1,4′]Bipiperidinyl-1′-yl-[(4S,5R)-2-(4-tert-butyl-2-ethoxy-phenyl)-4,5-bis-(4-chloro-phenyl)-4,5-dihydro-imidazol-1-yl]-methanone was prepared from (4S,5R)-2-(4-tert-butyl-2-ethoxy-phenyl)-4,5-bis-(4-chloro-phenyl)-4,5-dihydro-imidazole-1-carbonyl chloride (example 11) and 4-piperidinopiperidine (Aldrich) in an analogous manner as described in example 25. HR-MS (ES, m/z): observed 661.3071, calculated for C38H47Cl2N4O3 [(M+H)+] 661.3071.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07964724B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-e159eda6adf244ad8abab4145ce4d712 |
| Source note | uspto-grants-2011_06 |