Iodoethane → (+/-)-Ethyl (3-ethyl-4-nitro-2-oxo-2,3-dihydro-1H-indol-3-yl)acetate

HRID 2426183Notes

Reaction equation

HRID 2426183 reaction equation
[CH3:1][C:2]1([CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][C:9]=2[N+:11]([O-:13])=[O:12])[NH:4][C:3]1=[O:14].I[CH2:22]C>>[CH2:1]([C:2]1([CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][C:9]=2[N+:11]([O-:13])=[O:12])[NH:4][C:3]1=[O:14])[CH3:22]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 86629726(-)-Ethyl (3-methyl-4-nitro-2-oxo-2,3-dihydro-1H-indol-3-yl)acetate

Product 1

HCID 86629733(+/-)-Ethyl (3-ethyl-4-nitro-2-oxo-2,3-dihydro-1H-indol-3-yl)acetate

Procedure

Essentially following the procedures described for Intermediate 16, but using iodoethane in place of iodomethane, the title compound was prepared. MS: m/z=293 (M+1).

Sources & evidence

ORD record
ord-7d6656f9202a473a97d6800e0cde57a4
Source dataset
uspto-grants-2011_06
Patent number
US07968540B2

Reaction notes

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