HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57863157, compound → HCID 57863140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57863157 | HCID 57863157 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 57863140 | HCID 57863140 | 73% |
Reaction Steps
10% Pd/C (0.29 g, 0.27 mmol) is added to 2-(1,3-benzodioxol-5-yl)-6-nitroquinoline (2.0 g, 6.80 mmol) in methanol/THF (80 ml/80 ml). The mixture is hydrogenated at r.t. for 2 hours. The catalyst is filtered off and the filtrate is concentrated to afford 1.31 g (73%) of the titled product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968558B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-8ac3c150816c4807a7fd4cc4376a2c04 |
| Source note | uspto-grants-2011_06 |