HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpiperidine → HCID 21105503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpiperidine | HCID 69381 | — |
| Reactant | HCID 10873809 | HCID 10873809 | — |
| Product | HCID 21105503 | HCID 21105503 | — |
Reaction Steps
Benzhydryl 5-trifluoromethanesulfonyloxypyridine-2-carboxylate (3.0 g) was heated with 4-methylpiperidine (1.4 g) at 80° C. for one hour. The reaction mixture was immediately purified by preparative HPLC and then hydrogenated in analogy to method. This resulted in the product with the molecular weight of 220.27 (C12H16N2O2); MS (ESI): 221 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968550B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-b93afa666fdf435a854a82aa9dd3f020 |
| Source note | uspto-grants-2011_06 |