HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → [4'-(Methanesulfonyl)[1,1'-biphenyl]-3-yl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 57787810 | HCID 57787810 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | [4'-(Methanesulfonyl)[1,1'-biphenyl]-3-yl]methanol | HCID 20100324 | — |
Reaction Steps
In an atmosphere of nitrogen, under ice-cooling, methyl 4′-(methylsulfonyl)biphenyl-3-carboxylate was added to a THF suspension of lithium aluminum hydride, followed by stirring for 20 minute to obtain [4′-(methylsulfonyl)biphenyl-3-yl]methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968552B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-5091657163d94514ae2854921c0f0b86 |
| Source note | uspto-grants-2011_06 |