Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 57787477 | HCID 57787477 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57787931 | HCID 57787931 | — |
Reaction Steps
Methanesulfonyl chloride was dropwise added under ice-cooling to a mixture of 4-[(4′-hydroxy-2′,6′-dimethylbiphenyl-3-yl)methoxy]benzaldehyde, triethylamine and ethyl acetate, followed by stirring at 0° C. for 2 hours to obtain 3′-[(4-formylphenoxy)methyl]-2,6-dimethylbiphenyl-4-yl methanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07968552B2 |
|---|
| Source dataset | uspto-grants-2011_06 |
|---|
| ORD ID | ord-71f8b1c3fc37457a834bd76c9720795e |
|---|
| Source note | uspto-grants-2011_06 |
|---|
