HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycol monoacetate → HCID 57422595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycol monoacetate | HCID 10960 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Bromo-5-fluorobenzotrifluoride | HCID 520983 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57422595 | HCID 57422595 | — |
Reaction Steps
In an atmosphere of nitrogen, a mixture of 2-hydroxyethyl acetate, sodium hydride and DMF was stirred at room temperature for 15 minutes and then 1-bromo-4-fluoro-2-(trifluoromethyl)benzene was added, followed by stirring at room temperature for 1.5 hours to obtain 2-[4-bromo-3-(trifluoromethyl)phenoxy]ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968552B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-911ab615685a4b86bd7485d79867b38c |
| Source note | uspto-grants-2011_06 |