HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57787091, compound → HCID 67252107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57787091 | HCID 57787091 | — |
| Reactant | HCID 178418373 | HCID 178418373 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67252107 | HCID 67252107 | — |
Reaction Steps
In an atmosphere of nitrogen, a THF solution of methylmagnesium iodide was dropwise added under ice-cooling to a THF solution of 1-[(3′-{[4-(hydroxymethyl)phenoxy]methyl}-2,6-dimethylbiphenyl-4-yl)oxy]acetone, followed by stirring at room temperature for 30 minute to obtain 1-[(3′-{[4-(hydroxymethyl)phenoxy]methyl}-2,6-dimethylbiphenyl-4-yl)oxy]-2-methylpropan-2-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968552B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-d5f4c59bf3e245af9962094f1cc7ae95 |
| Source note | uspto-grants-2011_06 |