Acetyl chloride → HCID 57787228, compound

HRID 2426768Notes

Reaction equation

HRID 2426768 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:11]=[C:10]([CH3:12])[C:9]([C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][O:20][C:21]3[CH:28]=[CH:27][C:24]([CH:25]=[O:26])=[CH:23][CH:22]=3)[C:14]=2C)=[CH:8][CH:7]=1.[C:30](Cl)(=[O:32])[CH3:31].[CH2:34](N(CC)CC)C>ClCCl>[C:30]([O:1][CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH3:34])[C:9]([C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][O:20][C:21]3[CH:28]=[CH:27][C:24]([CH:25]=[O:26])=[CH:23][CH:22]=3)[CH:14]=2)=[C:10]([CH3:12])[CH:11]=1)(=[O:32])[CH3:31]

Participants

5

Reactant 3

HCID 6367Acetyl chlorideHCID 8471TriethylamineHCID 57787450HCID 57787450, compound

Product 1

HCID 57787228HCID 57787228, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of 4-{[4′-(3-hydroxypropoxy)-2,6′-dimethylbiphenyl-3-yl]methoxy}benzaldehyde, acetyl chloride, triethylamine and dichloromethane was stirred at room temperature for 3.5 hours to obtain 3-({3′-[(4-formylphenoxy)methyl]-2,6-dimethylbiphenyl-4-yl}oxy)propyl acetate.

Sources & evidence

ORD record
ord-4ab34478101c4f528146d5a987f1655e
Source dataset
uspto-grants-2011_06
Patent number
US07968552B2

Reaction notes

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