Pyridine → HCID 57787618, compound

HRID 2426769Notes

Reaction equation

HRID 2426769 reaction equation
[OH:1][C:2]([CH3:31])([CH3:30])[CH2:3][CH2:4][O:5][C:6]1[CH:11]=[C:10]([CH3:12])[C:9]([C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][O:20][C:21]3[CH:28]=[CH:27][C:24]([CH:25]=[O:26])=[CH:23][CH:22]=3)[CH:14]=2)=[C:8]([CH3:29])[CH:7]=1.[C:32](OC(=O)C)(=[O:34])[CH3:33].N1C=CC=CC=1>CN(C1C=CN=CC=1)C.C(Cl)(Cl)Cl>[C:32]([O:1][C:2]([CH3:31])([CH3:30])[CH2:3][CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH3:29])[C:9]([C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][O:20][C:21]3[CH:22]=[CH:23][C:24]([CH:25]=[O:26])=[CH:27][CH:28]=3)[CH:14]=2)=[C:10]([CH3:12])[CH:11]=1)(=[O:34])[CH3:33]

Participants

6

Reactant 3

HCID 1049PyridineHCID 7918Acetic AnhydrideHCID 57787704HCID 57787704, compound

Product 1

HCID 57787618HCID 57787618, compound

Reagents, catalysts & solvents 2

HCID 142844-(Dimethylamino)pyridineCatalystHCID 6212ChloroformSolvent

Procedure

A mixture of 4-{[4′-(3-hydroxy-3-methylbutoxy)-2′,6′-dimethylbiphenyl-3-yl]methoxy}benzaldehyde, acetic anhydride, pyridine, DMAP and chloroform was stirred at room temperature for 2 days to obtain 3-({3′-[(4-formylphenoxy)methyl]-2,6-dimethylbiphenyl-4-yl}oxy)-1,1-dimethylpropyl acetate.

Sources & evidence

ORD record
ord-c34a5a3833e9463ba1059d1af17c8581
Source dataset
uspto-grants-2011_06
Patent number
US07968552B2

Reaction notes

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