HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 86639850, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | (2S)-2,3-Dihydroxy-N-methoxy-2,N-dimethyl-propionamide | HCID 11480618 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86639850 | HCID 86639850 | 102.2% |
Reaction Steps
To a solution of the compound prepared in Example 130(a) (565 mg) in methanol (7.0 mL) was added lithium hydroxide monohydrate (146 mg) and the mixture was stirred at room temperature for 4 hours. The reaction mixture was concentrated to give the title compound (446 mg) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968572B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-640a161f041a452882254f3fe9009af5 |
| Source note | uspto-grants-2011_06 |