HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-napthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2-Naphthalenethiol | HCID 7058 | — |
| Reactant | 3,4,5-Trichloronitrobenzene | HCID 88365 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-napthalene | HCID 22148877 | — |
Reaction Steps
2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-napthalene was synthesized (100%) from 3,4,5-trichloronitrobenzene (Acros) and napthalene-2-thiol (Avocado) in a similar manner as described in example 1 using DMSO as solvent instead of DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968567B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-b8b69190b50c4633a2db8d8662e5b825 |
| Source note | uspto-grants-2011_06 |