HRID2427220

反应详情

EQUATION

反应方程式

HRID 2427220 的结构方程式

PROCEDURE

实验过程

The title compound was prepared using the method of example 270, starting with 2-(2-chloro-4-nitro-phenylsulfanyl)-benzothiazole-6-carbonitrile (261) (1.6 g, 4.6 mmol), tin chloride dihydrate (Aldrich, 5.21 g, 23.1 mmol). Compound 273 (1.36 g, 93%) was obtained as a yellowish solid. MS (M+H) 318.

WORKUP

后处理

  1. customThe title compound was prepared