HRID2427235

反应详情

EQUATION

反应方程式

HRID 2427235 的结构方程式

PROCEDURE

实验过程

The title compound was prepared using the method of example 239, starting with 2-bromo-4-methyl-phenylamine (Acros) (27.9 g), O-ethylxanthic acid, potassium salt (Lancaster, 54 g) in DMF (250 mL). The mercaptobenzothiazole 340 was obtained as an pale brown solid (27 g). Recrystalization from CHCl3 gave pinkish white crystals (20 g).

WORKUP

后处理

  1. customThe title compound was prepared