HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Amino-1-hexanol → HCID 67262989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Amino-1-hexanol | HCID 19960 | — |
| Reactant | Trolox | HCID 40634 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Product | HCID 67262989 | HCID 67262989 | 23% |
Reaction Steps
Following the amide coupling procedure described in protocol A, 500 mg 6-hydroxy-2,5,7,8-tetramethylchroman-2-carboxylic acid (2.0 mmol), 356 mg CDI (2.2 mmol) and 468 mg 6-amino-1-hexanol (4.0 mmol) yielded 161 mg of 6-hydroxy-N-(6-hydroxyhexyl)-2,5,7,8-tetramethylchroman-2-carboxamide as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07968746B2 |
| Source dataset | uspto-grants-2011_06 |
| ORD ID | ord-012e860874674453a37dc7643fc9a0e6 |
| Source note | uspto-grants-2011_06 |