HRID24307
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
5-Fluoroisatin (8.2 g) was dissolved in 50 mL of hydrazine hydrate and refluxed for 1.0 hr. The reaction mixtures were then poured in ice water. The precipitate was then filtered, washed with water and dried in a vacuum oven to afford the title compound.
WORKUP
后处理
- temperaturerefluxed for 1.0 hr
- customThe reaction mixtures
- filtrationThe precipitate was then filtered
- washwashed with water
- customdried in a vacuum oven