HRID24310

反应详情

EQUATION

反应方程式

HRID 24310 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

5-Chlorosulfonyl-2-oxindole (2.1 g) was added to 10 mL of ammonium hydroxide in 10 mL of ethanol and stirred at room temperature overnight. The mixture was concentrated and the solid collected by vacuum filtration to give 0.4 g (20% yield) of the title compound as an off-white solid.

WORKUP

后处理

  1. concentrationThe mixture was concentrated
  2. filtrationthe solid collected by vacuum filtration