HCID 68157595, compound → HCID 68157564, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of (5-fluoro-2-nitrophenyl)-(2-methyl-2H-pyrazol-3-yl)-amine (0.96 g, 4.06 mmol) and 10% palladium on carbon (0.20 g) in EtOAc (40 mL) was stirred under an atmosphere of hydrogen at atmospheric pressure and 20° C. for 5 h. The catalyst was removed by filtration and the filtrate concentrated in vacuo to give the title compound as a white solid (0.63 g, 88%). LCMS (Method C): RT 1.88 min [M+H]+ 207.0

Provenance & Evidence