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HRID243626

反应详情

EQUATION

反应方程式

HRID 243626 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)CCCCCCC(=O)Nc1nc(-c2cccc([N+](=O)[O-])c2)cs1
HCID16733292

未命名化合物

结构：COC(=O)CCCCCCC(=O)Nc1nc(-c2cccc(N)c2)cs1
HCID44550930

octanedioic acid [4-(3-Amino-phenyl)-thiazol-2-yl]-amide methyl ester

C18H23N3O3S

PRODUCTS

生成物

1
结构：Nc1cccc(-c2csc(NC(=O)CCCCCCC(=O)O)n2)c1
HCID53323224

未命名化合物

PROCEDURE

实验过程

Compound 21 was prepared using the methodology described for the preparation of compound 18, by substituting compound 14 with compound 20. Yield (0.276 g, 79.8%). 1H NMR (300 MHz, CDCl3) δ 7.21 (1H, t, J=7.7 Hz), 7.07 (1H, d, J=8.2 Hz), 6.99 (2H, s), 6.69 (1H, d, J=7.8 Hz), 2.49 (2H, t, J=7.3 Hz), 2.40 (2H, t, J=7.1 Hz), 1.78 (2H, brs), 1.69 (2H, t, J=6.7 Hz), 1.50-1.35 (4H, m). 13C NMR (75 MHz, CDCl3) δ 179.6, 172.2, 160.8, 149.7, 147.1, 135.0, 130.2, 117.3, 115.6, 113.5, 108.1, 36.7, 34.4, 29.1, 28.9, 25.5, 24.9.

WORKUP

后处理

  1. customYield (0.276 g, 79.8%)