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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 243946Generated: October 27, 2026

HCID 67116252, compound → HCID 178519507, compound

https://huagongshe.com/reaction/243946

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67116252HCID 67116252—
ReactantHCID 178524291HCID 178524291—
ProductHCID 178519507HCID 178519507—

Reaction Steps

The title compound was prepared in a manner analogous to Example 15 utilizing Intermediate 30 and 2-(4H-[1,2,4]triazol-3-yl)-benzoic acid. MS (ESI) mass calcd. for C24H20F4N7O, 479.47; m/z found, 480.2 [M+H]+. 1H NMR (CDCl3): 8.12-7.93 (m, 3H), 7.77 (dd, J=8.5, 0.9 Hz, 1H), 7.69 (ddd, J=8.4, 6.8, 1.4 Hz, 1H), 7.52-7.41 (m, 3H), 7.38-7.34 (m, 1H), 4.01-3.79 (m, 3H), 3.78-3.66 (m, 2H), 3.49 (dd, J=23.0, 15.0 Hz, 2H), 3.16-2.88 (m, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08653263B2
Source datasetuspto-grants-2014_02
ORD IDord-ff21b18afe4640afb3df9149f307117f
Source noteuspto-grants-2014_02