HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-6-(2-pyrimidinyl)benzoic acid → HCID 67116482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-6-(2-pyrimidinyl)benzoic acid | HCID 67086603 | — |
| Reactant | [4-(Hexahydro-pyrrolo[3,4-c]pyrrol-2-yl)-6-trifluoromethyl-pyrimidin-2-yl]-dimethyl-amine | HCID 67116323 | — |
| Product | HCID 67116482 | HCID 67116482 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Example 15 utilizing Intermediate 36 and Intermediate 14. MS (ESI): mass calculated for C24H23F4N7O, 501.49; m/z found 502.0 [M+H]+. 1H NMR (400 MHz, CDCl3): 8.86-8.63 (m, 2H), 8.22-8.05 (m, 1H), 7.56-7.40 (m, 1H), 7.29-7.18 (m, 1H), 7.12 (br s, 1H), 6.03-5.73 (m, 1H), 4.19-2.90 (m, 16H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653263B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-17d7ec8fee2d472990bfba87fb1b176c |
| Source note | uspto-grants-2014_02 |