HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-6-(2H-1,2,3-triazol-2-yl)benzoic acid → HCID 69939595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-6-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086627 | — |
| Reactant | 2-(4,6-Dimethoxy-pyrimidin-2-yl)-octahydro-pyrrolo[3,4-c]pyrrole | HCID 67116491 | — |
| Product | HCID 69939595 | HCID 69939595 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Example 15, utilizing Intermediate 45 and Intermediate 12. MS (ESI): mass calculated for C21H22FN7O3, 439.18; m/z found 440.2 [M+H]+. 1H NMR (400 MHz, CDCl3): 7.89-7.80 (m, 2H), 7.73 (s, 1H), 7.53-7.43 (m, 1H), 7.15 (tdd, J=8.4, 3.7, 0.9, 1H), 5.39 (d, J=2.4, 1H), 4.02-3.48 (m, 13H), 3.31-2.89 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653263B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-1476b5fe360d42bea3aa55b66ada544d |
| Source note | uspto-grants-2014_02 |