HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86652717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Aminopyrene | HCID 15352 | — |
| Reactant | Ethyl 6-bromohexanoate | HCID 117544 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86652717 | HCID 86652717 | — |
Reaction Steps
A mixture of 1-aminopyrene (5 g), potassium carbonate (15 g) and ethyl 6-bromohexanoate (10 g) in 60 mL acetonitrile was refluxed for 24 hours. The solvent was removed and the product was purified by a silica gel column eluting with EtOAc/hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08658434B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-f03269c70b7b45c8a06a84ef212488cc |
| Source note | uspto-grants-2014_02 |