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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 244328Generated: October 30, 2026

HCID 58241683, compound → HCID 58241679, compound

https://huagongshe.com/reaction/244328

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58241683HCID 58241683—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 58241679HCID 5824167978.8%

Reaction Conditions

Temperature50 °C

Reaction Steps

Pd/C (0.1 g) was added to 2,6-dimethoxy-2′-methyl-3-nitrobiphenyl (0.2 g, 0.73 mmol) in methanol (20 ml), and under 1 atm of Hz, the mixture was heated at 50° C. for 2 h. Filtration and concentration gave 2,6-dimethoxy-2′-methylbiphenyl-3-ylamine (0.14 g) as a colorless oil, which was directly reacted further.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08658569B2
Source datasetuspto-grants-2014_02
ORD IDord-4da89c1414974d339722f7ecaa2d2e04
Source noteuspto-grants-2014_02