HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 244328Generated: October 30, 2026
HCID 58241683, compound → HCID 58241679, compound
https://huagongshe.com/reaction/244328
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 58241683 | HCID 58241683 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58241679 | HCID 58241679 | 78.8% |
Reaction Steps
Pd/C (0.1 g) was added to 2,6-dimethoxy-2′-methyl-3-nitrobiphenyl (0.2 g, 0.73 mmol) in methanol (20 ml), and under 1 atm of Hz, the mixture was heated at 50° C. for 2 h. Filtration and concentration gave 2,6-dimethoxy-2′-methylbiphenyl-3-ylamine (0.14 g) as a colorless oil, which was directly reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08658569B2 |
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| Source dataset | uspto-grants-2014_02 |
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| ORD ID | ord-4da89c1414974d339722f7ecaa2d2e04 |
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| Source note | uspto-grants-2014_02 |
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