HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58579589, compound → HCID 58579582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58579589 | HCID 58579589 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58579582 | HCID 58579582 | — |
Reaction Steps
To a solution of tert-butyl (4-nitrophenyl)(pyridin-2-ylmethyl)carbamate, 11a, (0.58 g, 1.76 mmol) in methanol (17 mL) was added Pd/C (50 mg) and an atmosphere of H2 was applied. After 14 h, the r×n was filtered through a plug of Celite and concentrated. The residue, 12a, was carried on without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08658650B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-81955ac9a9c9471da22b8cf800f32cf9 |
| Source note | uspto-grants-2014_02 |