Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 244510Generated: October 31, 2026

HCID 58579589, compound → HCID 58579582, compound

https://huagongshe.com/reaction/244510

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58579589HCID 58579589—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 58579582HCID 58579582—

Reaction Steps

To a solution of tert-butyl (4-nitrophenyl)(pyridin-2-ylmethyl)carbamate, 11a, (0.58 g, 1.76 mmol) in methanol (17 mL) was added Pd/C (50 mg) and an atmosphere of H2 was applied. After 14 h, the r×n was filtered through a plug of Celite and concentrated. The residue, 12a, was carried on without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08658650B2
Source datasetuspto-grants-2014_02
ORD IDord-81955ac9a9c9471da22b8cf800f32cf9
Source noteuspto-grants-2014_02