Lithium Hydroxide → HCID 67115305, compound

HRID 244515Notes

Reaction equation

HRID 244515 reaction equation
[S:1]1[CH:5]=[CH:4][N:3]=[C:2]1[N:6]1[CH2:11][CH2:10][CH:9]([C:12]([O:14]CC)=[O:13])[CH2:8][CH2:7]1.[Li+:17].[OH-]>CO>[S:1]1[CH:5]=[CH:4][N:3]=[C:2]1[N:6]1[CH2:11][CH2:10][CH:9]([C:12]([O-:14])=[O:13])[CH2:8][CH2:7]1.[Li+:17]

Participants

4

Reactant 2

HCID 3939Lithium HydroxideHCID 60658779HCID 60658779, compound

Product 1

HCID 67115305HCID 67115305, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a methanol (30 mL) solution of 3 (3.6 g, 15 mmol) was added LiOH solution (1.0 M, 15 mL) at room temperature. The resulting solution was stirred overnight and then concentrated to yield a solid as 4.

Workup

  1. concentrationconcentrated
  2. customto yield a solid as 4

Sources & evidence

ORD record
ord-94a7e0b918bb4a568deb65f7c3bc53fb
Source dataset
uspto-grants-2014_02
Patent number
US08658651B2

Reaction notes

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