Benzaldehyde → HCID 11965522, compound

Participants

Reaction Steps

To a stirred solution of 4-[2-(5-Acetyl-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile (100 mg, 0.315 mmol) and benzaldehyde (0.035 mL, 0.35 mmol) in ethanol, was added dropwise at 0° C., 1 mL of aqueous NaOH 30%. After the mixture was stirred at room temperature for 16 h and poured into ice water (ca. 10 mL). The precipitate was filtered, washed diethyl ether and dried under vacuum.

Provenance & Evidence