Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 244619Generated: October 31, 2026

Hydrochloric Acid → HCID 19619889, compound

https://huagongshe.com/reaction/244619

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 50896795HCID 50896795—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 19619889HCID 19619889100.3%

Reaction Conditions

Temperature105 °C

Reaction Steps

To a solution of methyl 4-chloro-1-(1-methylethyl)-1H-pyrazole-3-carboxylate (105 mg) in 1,4-dioxane (3 ml) was added 2M hydrochloric acid (3 ml) and the mixture heated at 105° C. for 18 h. The solvent was removed in vacuo to give the title compound as a yellow oil (98 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08658635B2
Source datasetuspto-grants-2014_02
ORD IDord-b216717d8a9f44fca9425a1d82a67ef7
Source noteuspto-grants-2014_02