HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[2-(benzyloxy)-5-(2-bromoacetyl)phenyl]methanesulfonamide → N-[2-Benzyloxy-5-[(2-ethyl-indan-2-ylamino)-acetyl]-phenyl]-methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[2-(benzyloxy)-5-(2-bromoacetyl)phenyl]methanesulfonamide | HCID 11200351 | — |
| Reactant | 2-ethyl-2,3-dihydro-1H-inden-2-amine | HCID 22499256 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-[2-Benzyloxy-5-[(2-ethyl-indan-2-ylamino)-acetyl]-phenyl]-methanesulfonamide | HCID 22499207 | — |
Reaction Steps
A mixture of 2-ethyl-indan-2-ylamine and N-(2-benzyloxy-5-bromoacetyl-phenyl)-methanesulfonamide is stirred in acetonitrile at room temperature for 20 hours. The product is isolated by filtration. ES+ MS m/e 479 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08658673B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-496149cb88364a15aaade637c5b159eb |
| Source note | uspto-grants-2014_02 |